Information card for entry 7027055

Structure parameters

• Formula: C55.5 H33 Cl O11 Os3 P2
• Calculated formula: C55.5 H32 Cl O11 Os3 P2
• Title of publication: Trinuclear clusters of osmium containing monodentate, chelating and orthometallated forms of 2,2′-bis(diphenylphosphino)-1,1′-binaphthyl (BINAP)
• Authors of publication: Deeming, Antony J.; Stchedroff, Marc
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 22
• Pages of publication: 3819
• a: 15.61 ± 0.004 Å
• b: 10.957 ± 0.002 Å
• c: 16.186 ± 0.004 Å
• α: 90°
• β: 108.97 ± 0.02°
• γ: 90°
• Cell volume: 2618.1 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0783
• Residual factor for significantly intense reflections: 0.0595
• Weighted residual factors for all reflections: 0.1611
• Weighted residual factors for significantly intense reflections: 0.1355
• Goodness-of-fit parameter for all reflections: 1.068
• Goodness-of-fit parameter for significantly intense reflections: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No