Information card for entry 7027441

Structure parameters

• Formula: C26 H40 O2 Sb2 Si2
• Calculated formula: C26 H40 O2 Sb2 Si2
• SMILES: O(C(=[Sb][Sb]=C(c1c(cc(cc1C)C)C)O[Si](C)(C)C)c1c(cc(cc1C)C)C)[Si](C)(C)C
• Title of publication: Compounds containing λ3,σ2-SbC bonds: synthesis and structural characterisation of the first stiba-enol, Mes*C(O)SbC(OH)Mes* (Mes* = C6H2But3-2,4,6) and a 2,3-distibabutadiene, {Mes(Me3SiO)CSb}2 (Mes = C6H2Me3-2,4,6) †
• Authors of publication: Jones, Cameron; Steed, Jonathan W.; Thomas, Ryan C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 10
• Pages of publication: 1541
• a: 10.704 ± 0.002 Å
• b: 14.043 ± 0.003 Å
• c: 10.889 ± 0.002 Å
• α: 90°
• β: 109.57 ± 0.03°
• γ: 90°
• Cell volume: 1542.2 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0482
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.094
• Weighted residual factors for all reflections included in the refinement: 0.1127
• Goodness-of-fit parameter for all reflections included in the refinement: 0.502
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No