Information card for entry 7027709

Structure parameters

• Formula: C146 H170 Cl16 O9 P4 Pt2
• Calculated formula: C146 H152 Cl16 O9 P4 Pt2
• Title of publication: Co-ordination chemistry of macrocyclic compounds with dangling phosphines. Unusual NMR shifts in metallo-calix[4]arenes †
• Authors of publication: Dieleman, Cedric B.; Marsol, Claire; Matt, Dominique; Kyritsakas, Nathalie; Harriman, Anthony; Kintzinger, Jean-Pierre
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 23
• Pages of publication: 4139
• a: 12.571 ± 0.001 Å
• b: 22.5546 ± 0.0003 Å
• c: 26.4894 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7510.6 ± 0.6 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.068
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for all reflections: 0.371
• Weighted residual factors for all reflections included in the refinement: 0.068
• Goodness-of-fit parameter for all reflections: 5.859
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No