Information card for entry 7027846

Structure parameters

• Formula: C76 H64 Mo2 N4 O6
• Calculated formula: C92 H48 Mo2 N4 O10
• Title of publication: Molybdenum‒carbon functionalities supported by a quadridentate Schiff-base ligand: the reactivity of trans-dichloro[N,N′-bis(salicylidene)-o-phenylenediaminato]molybdenum(IV) ‡
• Authors of publication: Solari, Euro; Maltese, Cristiano; Latronico, Mario; Floriani, Carlo; Chiesi-Villa, Angiola; Rizzoli, Corrado
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 14
• Pages of publication: 2395
• a: 24.185 ± 0.004 Å
• b: 14.435 ± 0.002 Å
• c: 17.044 ± 0.002 Å
• α: 90 ± 0°
• β: 90 ± 0°
• γ: 90 ± 0°
• Cell volume: 5950.2 ± 1.5 ų
• Cell temperature: 25 K
• Ambient diffraction temperature: 133 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1109
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for all reflections: 0.1209
• Weighted residual factors for significantly intense reflections: 0.1047
• Goodness-of-fit parameter for all reflections: 1.058
• Goodness-of-fit parameter for significantly intense reflections: 1.14
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No