Information card for entry 7027915

Structure parameters

• Formula: C18 H22 N2 O4 W
• Calculated formula: C18 H22 N2 O4 W
• Title of publication: cis-Dioxo-tungsten(VI) and -molybdenum(VI) complexes with N2O2 tetradentate ligands: synthesis, structure, electrochemistry and oxo-transfer properties
• Authors of publication: Wong, Yee-Lok; Yan, Yan; Chan, Edith S. H.; Yang, Qingchuan; Mak, Thomas C. W.; Ng, Dennis K. P.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 18
• Pages of publication: 3057
• a: 19.015 ± 0.0014 Å
• b: 7.4238 ± 0.0005 Å
• c: 14.894 ± 0.0011 Å
• α: 90°
• β: 119.4 ± 0.004°
• γ: 90°
• Cell volume: 1831.7 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0539
• Weighted residual factors for all reflections: 0.166
• Weighted residual factors for significantly intense reflections: 0.1453
• Goodness-of-fit parameter for all reflections: 1.05
• Goodness-of-fit parameter for significantly intense reflections: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No