Information card for entry 7028187

Structure parameters

• Common name: [Ni(cdsalpd)]
• Formula: C17 H20 N2 Ni O S2
• Calculated formula: C17 H20 N2 Ni O S2
• Title of publication: Synthesis, spectroscopic and electrochemical study of nickel-(II) and -(I) complexes with Schiff-base ligands giving a NN′OS co-ordination sphere
• Authors of publication: Pereira, Eulália; Gomes, Lígia; Castro, Baltazar de
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 4
• Pages of publication: 629
• a: 8.924 ± 0.005 Å
• b: 16.889 ± 0.008 Å
• c: 12.051 ± 0.006 Å
• α: 90°
• β: 97.94 ± 0.02°
• γ: 90°
• Cell volume: 1798.9 ± 1.6 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0333
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for all reflections: 0.0749
• Weighted residual factors for significantly intense reflections: 0.0687
• Goodness-of-fit parameter for all reflections: 1.058
• Goodness-of-fit parameter for significantly intense reflections: 1.059
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No