Information card for entry 7028664

Structure parameters

• Common name: [(EtOH)DiPPIm]2AgCl
• Formula: C35 H50 Ag Cl3 N4 O2
• Calculated formula: C35 H50 Ag Cl3 N4 O2
• Title of publication: Synthesis and characterization of oxygen-functionalised-NHC silver(i) complexes and NHC transmetallation to nickel(ii).
• Authors of publication: Hameury, Sophie; de Frémont, Pierre; R Breuil, Pierre-Alain; Olivier-Bourbigou, Hélène; Braunstein, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 12
• Pages of publication: 4700 - 4710
• a: 19.5798 ± 0.0005 Å
• b: 19.7314 ± 0.0009 Å
• c: 12.239 ± 0.0005 Å
• α: 90°
• β: 126.049 ± 0.002°
• γ: 90°
• Cell volume: 3823 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0634
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1213
• Weighted residual factors for all reflections included in the refinement: 0.1465
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No