Information card for entry 7028895

Structure parameters

• Formula: C16 H19 O6 P W
• Calculated formula: C16 H19 O6 P W
• SMILES: CO[PH](C1(C(=C(C(=C1C)C)C)C)C)[W](C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Synthesis of Li/OR phosphinidenoid complexes: on the evidence for intramolecular O-Li donation and the effect of cation encapsulation.
• Authors of publication: Streubel, Rainer; Kyri, Andreas Wolfgang; Duan, Lili; Schnakenburg, Gregor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 5
• Pages of publication: 2088 - 2097
• a: 8.5181 ± 0.0005 Å
• b: 8.6529 ± 0.0005 Å
• c: 13.6246 ± 0.0008 Å
• α: 93.925 ± 0.005°
• β: 99.505 ± 0.005°
• γ: 108.288 ± 0.004°
• Cell volume: 932.62 ± 0.1 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0206
• Residual factor for significantly intense reflections: 0.0199
• Weighted residual factors for significantly intense reflections: 0.0512
• Weighted residual factors for all reflections included in the refinement: 0.0515
• Goodness-of-fit parameter for all reflections included in the refinement: 1.102
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No