Crystallography Open Database

Information card for entry 7029266

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Coordinates	7029266.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H59 Li N2 O2 Sn
Calculated formula	C38 H50 Li N2 O2 Sn
Title of publication	Benzannulated N-heterocyclic germylenes and stannylenes with sterically demanding N,N'-substituents.
Authors of publication	Krupski, Sergei; Pöttgen, Rainer; Schellenberg, Inga; Hahn, F. Ekkehardt
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	1
Pages of publication	173 - 181
a	10.7805 ± 0.0004 Å
b	11.2513 ± 0.0004 Å
c	14.5939 ± 0.0006 Å
α	97.029 ± 0.001°
β	95.415 ± 0.001°
γ	94.351 ± 0.001°
Cell volume	1742.16 ± 0.11 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0441
Residual factor for significantly intense reflections	0.0391
Weighted residual factors for significantly intense reflections	0.1068
Weighted residual factors for all reflections included in the refinement	0.1104
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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