Information card for entry 7029731

Structure parameters

• Formula: C44 H65 N P Si2 Y
• Calculated formula: C44 H65 N P Si2 Y
• Title of publication: Tetrahydropentalenyl-phosphazene constrained geometry complexes of rare-earth metal alkyls.
• Authors of publication: Hangaly, Noa K; Petrov, Alexander R; Elfferding, Michael; Harms, Klaus; Sundermeyer, Jörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 19
• Pages of publication: 7109 - 7120
• a: 19.4018 ± 0.0013 Å
• b: 20.3212 ± 0.0012 Å
• c: 23.1462 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9125.8 ± 1 ų
• Cell temperature: 466 ± 2 K
• Ambient diffraction temperature: 466 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0918
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0683
• Weighted residual factors for all reflections included in the refinement: 0.0981
• Goodness-of-fit parameter for all reflections included in the refinement: 0.829
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No