Information card for entry 7029848

Structure parameters

• Formula: C75 H110 B2 N6 O12 Os P4
• Calculated formula: C75 H110 B2 N6 O12 Os P4
• SMILES: [Os]1([NH2]N(C(=[NH]1)N=C(N)N)C)([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)[P](OCC)(OCC)OCC.[B-](c1ccccc1)(c1ccccc1)(c1ccccc1)c1ccccc1.[B-](c1ccccc1)(c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Preparation and reactivity towards hydrazines of bis(cyanamide) and bis(cyanoguanidine) complexes of the iron triad.
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Caia, Alfonso; Castro, Jesús
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 19
• Pages of publication: 7314 - 7323
• a: 17.0333 ± 0.0013 Å
• b: 20.4889 ± 0.0016 Å
• c: 24.4972 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8549.4 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.159
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.087
• Weighted residual factors for all reflections included in the refinement: 0.1185
• Goodness-of-fit parameter for all reflections included in the refinement: 0.954
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No