Information card for entry 7030114

Structure parameters

• Formula: C15 H29 K N4
• Calculated formula: C14.997 H29 K N4
• Title of publication: Lithium, sodium and potassium picolyl complexes: syntheses, structures and bonding.
• Authors of publication: Kennedy, Alan R.; Mulvey, Robert E.; Urquhart, Robert I.; Robertson, Stuart D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 38
• Pages of publication: 14265 - 14274
• a: 9.177 ± 0.0006 Å
• b: 10.2187 ± 0.0008 Å
• c: 10.7465 ± 0.0007 Å
• α: 107.162 ± 0.007°
• β: 93.767 ± 0.005°
• γ: 105.164 ± 0.007°
• Cell volume: 918.15 ± 0.12 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0565
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.1001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No