Information card for entry 7030226

Structure parameters

• Formula: C40 H38 Cl4 N3 Ni O P
• Calculated formula: C40 H38 Cl4 N3 Ni O P
• Title of publication: Nickel complexes supported by quinoline-based ligands: synthesis, characterization and catalysis in the cross-coupling of arylzinc reagents and aryl chlorides or aryltrimethylammonium salts.
• Authors of publication: Zhang, Qiang; Zhang, Xue-Qi; Wang, Zhong-Xia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 34
• Pages of publication: 10453 - 10464
• a: 11.4343 ± 0.0015 Å
• b: 11.602 ± 0.0015 Å
• c: 17.1801 ± 0.0019 Å
• α: 76.682 ± 0.002°
• β: 73.197 ± 0.001°
• γ: 64.542 ± 0.001°
• Cell volume: 1955.1 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1415
• Residual factor for significantly intense reflections: 0.0858
• Weighted residual factors for significantly intense reflections: 0.1953
• Weighted residual factors for all reflections included in the refinement: 0.2113
• Goodness-of-fit parameter for all reflections included in the refinement: 1.309
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No