Information card for entry 7030228

Structure parameters

• Formula: C107 H90 Cl2 N8 Ni2 P4
• Calculated formula: C107 H90 Cl2 N8 Ni2 P4
• Title of publication: Nickel complexes supported by quinoline-based ligands: synthesis, characterization and catalysis in the cross-coupling of arylzinc reagents and aryl chlorides or aryltrimethylammonium salts.
• Authors of publication: Zhang, Qiang; Zhang, Xue-Qi; Wang, Zhong-Xia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 34
• Pages of publication: 10453 - 10464
• a: 11.7609 ± 0.0014 Å
• b: 12.4767 ± 0.0016 Å
• c: 17.359 ± 0.0018 Å
• α: 82.372 ± 0.001°
• β: 85.171 ± 0.002°
• γ: 79.23 ± 0.001°
• Cell volume: 2475.6 ± 0.5 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0945
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1716
• Weighted residual factors for all reflections included in the refinement: 0.1936
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No