Information card for entry 7030275

Structure parameters

• Chemical name: trans-tetrafluoro-bis(triphenylarsine oxide)-zirconium(IV) dichloromethane solvate
• Formula: C38 H34 As2 Cl4 F4 O2 Zr
• Calculated formula: C38 H34 As2 Cl4 F4 O2 Zr
• Title of publication: Preparation and structures of coordination complexes of the very hard Lewis acids ZrF4 and HfF4.
• Authors of publication: Benjamin, Sophie L.; Levason, William; Pugh, David; Reid, Gillian; Zhang, Wenjian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 40
• Pages of publication: 12548 - 12557
• a: 8.898 ± 0.003 Å
• b: 14.688 ± 0.004 Å
• c: 14.84 ± 0.005 Å
• α: 90°
• β: 94.348 ± 0.007°
• γ: 90°
• Cell volume: 1933.9 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0746
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for significantly intense reflections: 0.1172
• Weighted residual factors for all reflections included in the refinement: 0.1261
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No