Information card for entry 7030356
| Formula |
C37 H46 Cl Fe N6 O6 |
| Calculated formula |
C37 H46 Cl Fe N6 O6 |
| Title of publication |
N-2-Hydroxybenzaldehyde acylhydrazone-Fe(iii) complex: synthesis, crystal structure and its efficient and selective N-methylation. |
| Authors of publication |
Li, Zhiyou; Wu, Lamei; Zhang, Tao; Huang, Zhengxi; Qiu, Guofu; Zhou, Zhongqiang; Jin, Longfei |
| Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
| Year of publication |
2014 |
| Journal volume |
43 |
| Journal issue |
20 |
| Pages of publication |
7554 - 7560 |
| a |
12.311 ± 0.004 Å |
| b |
13.132 ± 0.004 Å |
| c |
14.299 ± 0.005 Å |
| α |
99.409 ± 0.004° |
| β |
108.611 ± 0.004° |
| γ |
98.761 ± 0.005° |
| Cell volume |
2109 ± 1.2 Å3 |
| Cell temperature |
150 ± 2 K |
| Ambient diffraction temperature |
150 ± 2 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.1335 |
| Residual factor for significantly intense reflections |
0.0888 |
| Weighted residual factors for significantly intense reflections |
0.2001 |
| Weighted residual factors for all reflections included in the refinement |
0.2299 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.986 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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