Information card for entry 7030607

Structure parameters

• Formula: C59 H74 Br4 Cl15 N6 Ni2 O2.5
• Calculated formula: C59 H69 Br4 Cl15 N6 Ni2 O2.5
• Title of publication: Bis(imino)quaterpyridine-bearing multimetallic late transition metal complexes as ethylene oligomerisation catalysts
• Authors of publication: Khamker, Qudsia; Champouret, Yohan D. M.; Singh, Kuldip; Solan, Gregory A.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 41
• Pages of publication: 8935 - 8944
• a: 17.709 ± 0.003 Å
• b: 16.267 ± 0.003 Å
• c: 27.122 ± 0.005 Å
• α: 90°
• β: 96.154 ± 0.004°
• γ: 90°
• Cell volume: 7768 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1344
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.1152
• Weighted residual factors for all reflections included in the refinement: 0.1345
• Goodness-of-fit parameter for all reflections included in the refinement: 0.88
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7002529
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No