Information card for entry 7030644

Structure parameters

• Formula: C33 H36 N6 Si Sn
• Calculated formula: C33 H36 N6 Si Sn
• SMILES: [Sn]([Si](n1nc(cc1C)C)(n1nc(cc1C)C)n1nc(cc1C)C)(c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Syntheses, structures, and reactivity of poly(pyrazolyl)silanes, -disilanes, and the ambidentate κ1Si/κ3N-coordinating tris(3,5-dimethylpyrazolyl)silanide ligand [Si(3,5-Me2pz)3]− (MeTpsd)
• Authors of publication: Armbruster, Felix; Fernández, Ignacio; Breher, Frank
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 29
• Pages of publication: 5612 - 5626
• a: 10.455 ± 0.002 Å
• b: 17.266 ± 0.004 Å
• c: 17.588 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3174.9 ± 1.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0494
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.0811
• Weighted residual factors for all reflections included in the refinement: 0.0875
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7001727
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No