Crystallography Open Database

Information card for entry 7030671

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Coordinates	7030671.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H106 N8 O14 Zn9
Calculated formula	C66 H106 N8 O14 Zn9
Title of publication	Unique formation of mono-, tetra- and nona-nuclear zinc complexes from protonolysis reactions of [Zn(dmpzm)Et2]
Authors of publication	Cheng, Mei-Ling; Li, Hong-Xi; Liu, Lei-Lei; Wang, Hui-Hui; Zhang, Yong; Lang, Jian-Ping
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	11
Pages of publication	2012 - 2019
a	23.993 ± 0.005 Å
b	13.776 ± 0.003 Å
c	15.394 ± 0.003 Å
α	90°
β	128.64 ± 0.03°
γ	90°
Cell volume	3974 ± 2 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0831
Residual factor for significantly intense reflections	0.0643
Weighted residual factors for significantly intense reflections	0.1308
Weighted residual factors for all reflections included in the refinement	0.1392
Goodness-of-fit parameter for all reflections included in the refinement	1.139
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7000750
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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