Information card for entry 7030785

Structure parameters

• Formula: C22 H35 Cl5 N Nb P4
• Calculated formula: C22 H35 Cl5 N Nb P4
• Title of publication: Soft diphosphine and diarsine complexes of niobium(v) and tantalum(v) fluorides: synthesis, properties, structures and comparisons with the corresponding chlorides.
• Authors of publication: Levason, William; Light, Mark E.; Reid, Gillian; Zhang, Wenjian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 25
• Pages of publication: 9557 - 9566
• a: 21.764 ± 0.006 Å
• b: 10.178 ± 0.002 Å
• c: 14.77 ± 0.004 Å
• α: 90°
• β: 109.431 ± 0.009°
• γ: 90°
• Cell volume: 3085.4 ± 1.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.065
• Weighted residual factors for all reflections included in the refinement: 0.0663
• Goodness-of-fit parameter for all reflections included in the refinement: 1.188
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No