Information card for entry 7030787

Structure parameters

• Formula: C22.5 H36 Cl9 N Nb2 O P4
• Calculated formula: C22.5 H36 Cl9 N Nb2 O P4
• Title of publication: Soft diphosphine and diarsine complexes of niobium(v) and tantalum(v) fluorides: synthesis, properties, structures and comparisons with the corresponding chlorides.
• Authors of publication: Levason, William; Light, Mark E.; Reid, Gillian; Zhang, Wenjian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 25
• Pages of publication: 9557 - 9566
• a: 15.733 ± 0.002 Å
• b: 14.914 ± 0.002 Å
• c: 32.08 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7527.3 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1042
• Residual factor for significantly intense reflections: 0.0745
• Weighted residual factors for significantly intense reflections: 0.1024
• Weighted residual factors for all reflections included in the refinement: 0.1111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.19
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No