Clathrochelates meet phosphorus: thiophosphorylation of Fe(ii) dichloroclathrochelate precursor, synthesis of N,S-donor macrobicyclic ligands and their Pd(ii) complexes as potent catalysts of Suzuki cross-coupling reaction.
Authors of publication
Artyushin, Oleg I.; Odinets, Irina L.; Matveeva, Ekaterina V.; Vologzhanina, Anna V.; Varzatskii, Oleg A.; Lyubimov, Sergey E.; Voloshin, Yan Z.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2014
Journal volume
43
Journal issue
25
Pages of publication
9677 - 9689
a
13.219 ± 0.014 Å
b
13.73 ± 0.02 Å
c
16.225 ± 0.018 Å
α
90.88 ± 0.04°
β
100.76 ± 0.03°
γ
112.68 ± 0.05°
Cell volume
2657 ± 6 Å3
Cell temperature
120 ± 0.2 K
Ambient diffraction temperature
120 ± 0.2 K
Number of distinct elements
10
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1059
Residual factor for significantly intense reflections
0.0644
Weighted residual factors for significantly intense reflections
0.1277
Weighted residual factors for all reflections included in the refinement
0.1462
Goodness-of-fit parameter for all reflections included in the refinement
