Limiting nuclearity in formation of polynuclear metal complexes through [2 + 3] cycloaddition: synthesis and magnetic properties of tri- and pentanuclear metal complexes.
Authors of publication
Saha, Manideepa; Nasani, Rajendar; Das, Mriganka; Mahata, Arup; Pathak, Biswarup; Mobin, Shaikh M.; Carrella, Luca M.; Rentschler, Eva; Mukhopadhyay, Suman
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2014
Journal volume
43
Journal issue
21
Pages of publication
8083 - 8093
a
11.0194 ± 0.0011 Å
b
12.2772 ± 0.0012 Å
c
12.34 ± 0.0013 Å
α
79.47 ± 0.008°
β
76.251 ± 0.009°
γ
79.852 ± 0.008°
Cell volume
1578.8 ± 0.3 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0702
Residual factor for significantly intense reflections
0.0536
Weighted residual factors for significantly intense reflections
0.142
Weighted residual factors for all reflections included in the refinement
0.1617
Goodness-of-fit parameter for all reflections included in the refinement
