Crystallography Open Database

Information card for entry 7031280

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Coordinates	7031280.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H54 Al N Si
Calculated formula	C30 H54 Al N Si
Title of publication	Hydrometallation of amino-trialkynylsilanes - intramolecular M-N interactions (M = Al, Ga) and potential activation of Si-N bonds.
Authors of publication	Uhl, Werner; Bohnemann, Jörg; Kappelt, Benedikt; Hepp, Alexander; Layh, Marcus
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	38
Pages of publication	14386 - 14398
a	28.5934 ± 0.0012 Å
b	15.1324 ± 0.0006 Å
c	18.5944 ± 0.0008 Å
α	90°
β	124.746 ± 0.001°
γ	90°
Cell volume	6610.9 ± 0.5 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0625
Residual factor for significantly intense reflections	0.0487
Weighted residual factors for significantly intense reflections	0.1328
Weighted residual factors for all reflections included in the refinement	0.1428
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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