Information card for entry 7031831

Structure parameters

• Formula: B36 Cs4 H53.6 K16 O140.8 V24
• Calculated formula: B36 Cs4 K16 O140.8 V24
• Title of publication: Crystal lattice effect on the quenching of the intracluster magnetic interaction in [V12B18O60H6](10-) polyoxometalate.
• Authors of publication: Hermosilla-Ibáñez, Patricio; Cañon-Mancisidor, Walter; Costamagna, Juan; Vega, Andrés; Paredes-García, Verónica; Garland, Maria Teresa; Le Fur, Eric; Cador, Olivier; Spodine, Evgenia; Venegas-Yazigi, Diego
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 37
• Pages of publication: 14132 - 14141
• a: 19.4188 ± 0.0014 Å
• b: 18.6745 ± 0.0014 Å
• c: 19.3128 ± 0.0014 Å
• α: 90°
• β: 91.944 ± 0.001°
• γ: 90°
• Cell volume: 6999.5 ± 0.9 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0837
• Residual factor for significantly intense reflections: 0.077
• Weighted residual factors for significantly intense reflections: 0.2264
• Weighted residual factors for all reflections included in the refinement: 0.2358
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No