Information card for entry 7031869

Structure parameters

• Chemical name: trans-diphenyl-bis(trimethylphosphine)nickel(ii)
• Formula: C18 H28 Ni P2
• Calculated formula: C18 H28 Ni P2
• Title of publication: Synthesis and structures of mononuclear 3,4-bis(trifluoromethyl)pyrrolyl complexes of Rh(i) and Ni(ii).
• Authors of publication: Rivers, Joseph H.; Jones, Richard A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 43
• Pages of publication: 16275 - 16282
• a: 6.3114 ± 0.0007 Å
• b: 8.6172 ± 0.001 Å
• c: 18.474 ± 0.002 Å
• α: 82.806 ± 0.004°
• β: 89.043 ± 0.005°
• γ: 68.545 ± 0.004°
• Cell volume: 927.29 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.032
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.0777
• Weighted residual factors for all reflections included in the refinement: 0.0798
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No