Information card for entry 7031987

Structure parameters

• Formula: C27 H25 Cl2 N3 O3 Pb
• Calculated formula: C27 H25 Cl2 N3 O3 Pb
• Title of publication: Distinguishable Zn(ii) and Pb(ii) template effects on forming pendant-armed Schiff-base macrocyclic complexes including a remarkable Pb(ii)-π macrocyclic complex.
• Authors of publication: Zhang, Kun; Geng, Jiao; Jin, Chao; Huang, Wei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 41
• Pages of publication: 15351 - 15358
• a: 10.404 ± 0.003 Å
• b: 10.422 ± 0.003 Å
• c: 13.66 ± 0.004 Å
• α: 98.637 ± 0.005°
• β: 102.317 ± 0.005°
• γ: 99.253 ± 0.004°
• Cell volume: 1401.9 ± 0.7 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0836
• Goodness-of-fit parameter for all reflections included in the refinement: 0.916
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No