Information card for entry 7032086

Structure parameters

• Chemical name: Piperazino-di-chloro-tri-piperazine-iron(II)
• Formula: C8 H20 Cl2 Fe N4
• Calculated formula: C8 H19 Cl2 Fe N4
• Title of publication: Tuning of the dimensional linkage from the complex to the framework by thermal conversion in the system Fe/Cl/piperazine.
• Authors of publication: Schönfeld, F; Wirthensohn, R.; Schmitt, H.-C.; Constantinidis, P.; Fischer, I.; Müller-Buschbaum, K
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 41
• Pages of publication: 15398 - 15406
• a: 7.146 ± 0.0013 Å
• b: 8.3668 ± 0.0016 Å
• c: 11.438 ± 0.002 Å
• α: 108.112 ± 0.006°
• β: 98.174 ± 0.006°
• γ: 101.691 ± 0.006°
• Cell volume: 620.8 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0315
• Residual factor for significantly intense reflections: 0.0274
• Weighted residual factors for significantly intense reflections: 0.0665
• Weighted residual factors for all reflections included in the refinement: 0.0691
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No