Information card for entry 7032694

Structure parameters

• Formula: C46 H86 N10 Nb2 O
• Calculated formula: C46 H86 N10 Nb2 O
• Title of publication: Mixed amido-/imido-/guanidinato niobium complexes: synthesis and the effect of ligands on insertion reactions.
• Authors of publication: Elorriaga, David; Carrillo-Hermosilla, Fernando; Antiñolo, Antonio; López-Solera, Isabel; Fernández-Galán, Rafael; Villaseñor, Elena
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 46
• Pages of publication: 17434 - 17444
• a: 13.279 ± 0.013 Å
• b: 17.841 ± 0.017 Å
• c: 22.19 ± 0.02 Å
• α: 90°
• β: 90.39 ± 0.018°
• γ: 90°
• Cell volume: 5257 ± 9 ų
• Cell temperature: 260 ± 2 K
• Ambient diffraction temperature: 260 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2973
• Residual factor for significantly intense reflections: 0.0838
• Weighted residual factors for significantly intense reflections: 0.1742
• Weighted residual factors for all reflections included in the refinement: 0.276
• Goodness-of-fit parameter for all reflections included in the refinement: 0.849
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No