Information card for entry 7032959

Structure parameters

• Formula: C32 H34 Mo24 N12 Na2 O83 P2 Zn8
• Calculated formula: C32 H28 Mo24 N12 Na2 O83 P2 Zn8
• Title of publication: Syntheses, structures and properties of two new organic-inorganic hybrid materials based on ε-Zn Keggin units {ε-PMo(V)8Mo(VI)4O(40-x)(OH)(x)Zn4}.
• Authors of publication: Miao, Hao; Hu, Gonghao; Guo, Jiuyu; Wan, Hongxiang; Mei, Hua; Zhang, Yu; Xu, Yan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 2
• Pages of publication: 694 - 700
• a: 13.138 ± 0.002 Å
• b: 14.569 ± 0.002 Å
• c: 14.778 ± 0.002 Å
• α: 61.985 ± 0.002°
• β: 87.646 ± 0.002°
• γ: 87.263 ± 0.002°
• Cell volume: 2493.8 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.074
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.1058
• Weighted residual factors for all reflections included in the refinement: 0.1161
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No