Information card for entry 7033019

Structure parameters

• Formula: C19.5 H31 K0.5 N2 O P0.5
• Calculated formula: C19.5 H31 K0.5 N2 O P0.5
• Title of publication: Cleavage of an aryl carbon-nitrogen bond of a phosphazido iron(II) complex promoted by hydride metathesis.
• Authors of publication: Ogawa, Takahiko; Suzuki, Tatsuya; Hein, Nicholas M.; Pick, Fraser S.; Fryzuk, Michael D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 1
• Pages of publication: 54 - 57
• a: 9.742 ± 0.002 Å
• b: 10.616 ± 0.002 Å
• c: 19.454 ± 0.005 Å
• α: 74.814 ± 0.005°
• β: 79.099 ± 0.005°
• γ: 84.049 ± 0.005°
• Cell volume: 1903.5 ± 0.7 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0765
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.158
• Weighted residual factors for all reflections included in the refinement: 0.1637
• Goodness-of-fit parameter for all reflections included in the refinement: 1.207
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No