Information card for entry 7033838

Structure parameters

• Formula: C33 H48 Cl4 Fe2 N8 Si2
• Calculated formula: C33 H48 Cl4 Fe2 N8 Si2
• SMILES: [Fe]12(N([Si](C)(C)C)C(=[N]3[Fe]([n]4c5c3cccc5ccc4C)(N([Si](C)(C)C)C(=[N]2c2c3[n]1c(ccc3ccc2)C)N(C)C)Cl)N(C)C)Cl.ClCCl
• Title of publication: Inserted products of lithium silylquinolylamide dimers [{8-(2-R-C9H5N)N(Me3Si)}Li·OEt2]2 (R = H or Me) with dimethylcyanamide and their reactive derivatives with metal halides.
• Authors of publication: Wang, Peng; Li, Haifen; Xue, Xiaoyan; Chen, Xia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 10
• Pages of publication: 4718 - 4725
• a: 15.103 ± 0.003 Å
• b: 15.635 ± 0.003 Å
• c: 17.934 ± 0.003 Å
• α: 90°
• β: 106.776 ± 0.002°
• γ: 90°
• Cell volume: 4054.6 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0562
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1109
• Weighted residual factors for all reflections included in the refinement: 0.1303
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No