Information card for entry 7033861

Structure parameters

• Formula: C34 H34 Cl6 N4 O2 Si
• Calculated formula: C33.998 H33.998 Cl5.994 N4 O2 Si
• Title of publication: Tp*Cu(i)-CN-SiL2-NC-Cu(i)Tp* - a hexacoordinate Si-complex as connector for redox active metals via π-conjugated ligands.
• Authors of publication: Kämpfe, Alexander; Brendler, Erica; Kroke, Edwin; Wagler, Jörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 10
• Pages of publication: 4744 - 4750
• a: 7.1083 ± 0.0006 Å
• b: 10.0939 ± 0.0009 Å
• c: 13.448 ± 0.0013 Å
• α: 92.222 ± 0.007°
• β: 96.813 ± 0.007°
• γ: 100.341 ± 0.007°
• Cell volume: 940.74 ± 0.15 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1059
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No