Information card for entry 7034047

Structure parameters

• Formula: C30 H45 Al N2
• Calculated formula: C30 H45 Al N2
• Title of publication: Synthesis, structural studies and ligand influence on the stability of aryl-NHC stabilised trimethylaluminium complexes.
• Authors of publication: Wu M, Melissa; Gill, Arran M.; Yunpeng, Lu; Falivene, Laura; Yongxin, Li; Ganguly, Rakesh; Cavallo, Luigi; García, Felipe
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 34
• Pages of publication: 15166 - 15174
• a: 16.6982 ± 0.0012 Å
• b: 19.5345 ± 0.0014 Å
• c: 19.2491 ± 0.0014 Å
• α: 90°
• β: 111.602 ± 0.003°
• γ: 90°
• Cell volume: 5837.9 ± 0.7 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1895
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.1602
• Weighted residual factors for all reflections included in the refinement: 0.2284
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No