Information card for entry 7034750

Structure parameters

• Formula: C124 H120 Br3 Cl19 P8 Pd4 S4
• Calculated formula: C124 H120 Br3 Cl19 P8 Pd4 S4
• Title of publication: Polydentate chalcogen reagents for the facile preparation of Pd2 and Pd4 complexes.
• Authors of publication: Azizpoor Fard, Mahmood; Willans, Mathew J.; Khalili Najafabadi, Bahareh; Levchenko, Tetyana I.; Corrigan, John F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 17
• Pages of publication: 8267 - 8277
• a: 17.875 ± 0.007 Å
• b: 26.862 ± 0.01 Å
• c: 26.933 ± 0.011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12932 ± 9 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.1846
• Weighted residual factors for all reflections included in the refinement: 0.2191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No