Crystallography Open Database

Information card for entry 7035034

Preview

Coordinates	7035034.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H63 B O3 P2 Ru
Calculated formula	C65 H63 B O3 P2 Ru
Title of publication	Preparation and reactivity of diazoalkane complexes of ruthenium stabilised by an indenyl ligand.
Authors of publication	Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; Dottorello, Gianluca
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	19
Pages of publication	9289 - 9303
a	11.8068 ± 0.0008 Å
b	13.0733 ± 0.0009 Å
c	19.3806 ± 0.0015 Å
α	108.948 ± 0.005°
β	89.64 ± 0.005°
γ	95.878 ± 0.005°
Cell volume	2813.3 ± 0.4 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1719
Residual factor for significantly intense reflections	0.1268
Weighted residual factors for significantly intense reflections	0.2831
Weighted residual factors for all reflections included in the refinement	0.3348
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7035034.html