Information card for entry 7035243

Structure parameters

• Common name: [Ni(phen)2]2Sn2S6*2.2'-bipy
• Chemical name: {[Ni(C12H8N2)2]2Sn2S6*C10H8N2
• Formula: C58 H40 N10 Ni2 S6 Sn2
• Calculated formula: C58 H40 N10 Ni2 S6 Sn2
• Title of publication: Utilization of mixtures of aromatic N-donor ligands of different coordination ability for the solvothermal synthesis of thiostannate containing molecules.
• Authors of publication: Hilbert, J.; Näther, C; Bensch, W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 25
• Pages of publication: 11542 - 11550
• a: 10.5715 ± 0.0002 Å
• b: 9.9086 ± 0.0002 Å
• c: 24.996 ± 0.0004 Å
• α: 90°
• β: 92.8 ± 0.001°
• γ: 90°
• Cell volume: 2615.17 ± 0.08 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.052
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1274
• Weighted residual factors for all reflections included in the refinement: 0.1307
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No