Information card for entry 7035269

Structure parameters

• Formula: C12 H72 La2 Li6 N2 Na4 O100 Sb2 W18
• Calculated formula: C12 H8 La2 N2 Na3.55 O78.5 Sb2 W18
• Title of publication: Construction of polyoxometalates from dynamic lacunary polyoxotungstate building blocks and lanthanide linkers.
• Authors of publication: Li, Lu-Lu; Han, Hua-Yan; Wang, Yong-Hui; Tan, Hua-Qiao; Zang, Hong-Ying; Li, Yang-Guang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 25
• Pages of publication: 11429 - 11436
• a: 18.6089 ± 0.0017 Å
• b: 24.713 ± 0.002 Å
• c: 25.418 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11689.3 ± 1.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 9
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0557
• Weighted residual factors for significantly intense reflections: 0.0843
• Weighted residual factors for all reflections included in the refinement: 0.0934
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No