Crystallography Open Database

Information card for entry 7035271

Preview

Coordinates	7035271.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H50 Li7 N2 Na3 O89 Pr2 Sb2 W18
Calculated formula	C12 H8 N2 Na2.5 O72 Pr2 Sb2 W18
Title of publication	Construction of polyoxometalates from dynamic lacunary polyoxotungstate building blocks and lanthanide linkers.
Authors of publication	Li, Lu-Lu; Han, Hua-Yan; Wang, Yong-Hui; Tan, Hua-Qiao; Zang, Hong-Ying; Li, Yang-Guang
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	25
Pages of publication	11429 - 11436
a	18.333 ± 0.004 Å
b	24.5 ± 0.005 Å
c	25.269 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	11350 ± 4 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	9
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.164
Residual factor for significantly intense reflections	0.0823
Weighted residual factors for significantly intense reflections	0.1297
Weighted residual factors for all reflections included in the refinement	0.1538
Goodness-of-fit parameter for all reflections included in the refinement	0.903
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7035271.html