Information card for entry 7035324

Structure parameters

• Formula: C36 H58 N8 O2 Sb2
• Calculated formula: C36 H58 N8 O2 Sb2
• SMILES: c1(c(cccc1C[N]12CCN(CC1)C)C[N]13CCN(CC1)C)[Sb]123O[Sb]23(c4c(cccc4C[N]42CCN(CC4)C)C[N]23CCN(CC2)C)O1
• Title of publication: A general route to monoorganopnicogen(iii) (M = Sb, Bi) compounds with a pincer (N,C,N) group and oxo ligands.
• Authors of publication: Strîmb, Gabriela; Pöllnitz, Alpár; Raţ, Ciprian I; Silvestru, Cristian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 21
• Pages of publication: 9927 - 9942
• a: 9.08 ± 0.002 Å
• b: 10.126 ± 0.003 Å
• c: 11.752 ± 0.003 Å
• α: 68.806 ± 0.004°
• β: 82.572 ± 0.004°
• γ: 83.749 ± 0.004°
• Cell volume: 996.7 ± 0.4 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0609
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for significantly intense reflections: 0.1056
• Weighted residual factors for all reflections included in the refinement: 0.1214
• Goodness-of-fit parameter for all reflections included in the refinement: 1.134
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No