Crystallography Open Database

Information card for entry 7035702

Preview

Coordinates	7035702.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C76 H86 Ag4 F24 N18 P4
Calculated formula	C76 H80 Ag4 F24 N18 P4
Title of publication	Synthesis of a flexible macrocyclic tetraimidazolium salt-precursor for a tetracarbene ligand with metal dependent coordination modes.
Authors of publication	Schulte To Brinke, Christian; Ekkehardt Hahn, F.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	32
Pages of publication	14315 - 14322
a	17.1961 ± 0.0006 Å
b	19.7707 ± 0.0006 Å
c	26.2271 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	8916.7 ± 0.5 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	72
Hermann-Mauguin space group symbol	I b a m
Hall space group symbol	-I 2 2c
Residual factor for all reflections	0.0591
Residual factor for significantly intense reflections	0.0498
Weighted residual factors for significantly intense reflections	0.1373
Weighted residual factors for all reflections included in the refinement	0.1505
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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