Information card for entry 7035924

Structure parameters

• Formula: C50 H59 K N3 P
• Calculated formula: C50 H59 K N3 P
• SMILES: [K+].P([N-]c1c(cc(cc1C(c1ccccc1)c1ccccc1)C(C)C)C(c1ccccc1)c1ccccc1)(N(CC)CC)N(CC)CC.Cc1ccccc1
• Title of publication: Extremely bulky secondary phosphinoamines as substituents for sterically hindered aminosilanes.
• Authors of publication: Böttcher, Tobias; Jones, Cameron
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 33
• Pages of publication: 14842 - 14853
• a: 18.506 ± 0.004 Å
• b: 12.825 ± 0.003 Å
• c: 18.632 ± 0.004 Å
• α: 90°
• β: 97.72 ± 0.03°
• γ: 90°
• Cell volume: 4382 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.105
• Residual factor for significantly intense reflections: 0.0776
• Weighted residual factors for significantly intense reflections: 0.2091
• Weighted residual factors for all reflections included in the refinement: 0.2331
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.7108 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No