Information card for entry 7036458

Structure parameters

• Formula: C18 H27 Li N2 O
• Calculated formula: C18 H27 Li N2 O
• Title of publication: Ring lithiation of 1,8-bis(dimethylamino)naphthalene: another side of the 'proton sponge coin'.
• Authors of publication: Antonov, Alexander S.; Pozharskii, Alexander F.; Ozeryanskii, Valery A.; Filarowski, Aleksander; Suponitsky, Kyrill Yu; Tolstoy, Peter M.; Vovk, Mikhail A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 40
• Pages of publication: 17756 - 17766
• a: 8.847 ± 0.004 Å
• b: 23.449 ± 0.009 Å
• c: 8.877 ± 0.004 Å
• α: 90°
• β: 108.188 ± 0.006°
• γ: 90°
• Cell volume: 1749.6 ± 1.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2494
• Residual factor for significantly intense reflections: 0.0847
• Weighted residual factors for significantly intense reflections: 0.1293
• Weighted residual factors for all reflections included in the refinement: 0.182
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No