Information card for entry 7036617

Structure parameters

• Formula: C56.4 H79.8 Cl4.8 F12 N6 Ni O3 Sb2
• Calculated formula: C56.4 H79.8 Cl4.8 F12 N6 Ni O3 Sb2
• Title of publication: X-ray structure of a Ni(ii)-tri-phenoxyl radical complex.
• Authors of publication: Benisvy, Laurent; Zats, Galina M.; Fleker, Ohad; Yufit, Dmitry S.; Orio, Maylis; Romanenko, Galina; Ovcharenko, Victor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 41
• Pages of publication: 17924 - 17926
• a: 15.0749 ± 0.0006 Å
• b: 15.0749 ± 0.0006 Å
• c: 54.398 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 10705.9 ± 0.7 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 8
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0538
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for significantly intense reflections: 0.1115
• Weighted residual factors for all reflections included in the refinement: 0.1178
• Goodness-of-fit parameter for all reflections included in the refinement: 1.175
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No