Copper(ii) tetrafluoroborate complexes with the N(3),N(4)-bridging coordination of 1-(tert-butyl)-1H-tetrazole: synthesis, crystal structure and magnetic properties.
Authors of publication
Degtyarik, Mikhail M.; Lyakhov, Alexander S.; Ivashkevich, Ludmila S.; Matulis, Vitaly E.; Matulis, Vadim E.; Gruschinski, Sina; Voitekhovich, Sergei V.; Kersting, Berthold; Ivashkevich, Oleg A.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2015
Journal volume
44
Journal issue
42
Pages of publication
18518 - 18526
a
11.2988 ± 0.0001 Å
b
12.5702 ± 0.0001 Å
c
12.5849 ± 0.0001 Å
α
89.7679 ± 0.0005°
β
76.6828 ± 0.0005°
γ
85.2409 ± 0.0005°
Cell volume
1733.14 ± 0.03 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0335
Residual factor for significantly intense reflections
0.0302
Weighted residual factors for significantly intense reflections
0.0803
Weighted residual factors for all reflections included in the refinement
0.0822
Goodness-of-fit parameter for all reflections included in the refinement
