Information card for entry 7036773

Structure parameters

• Formula: H126 K11 Li23 O250 P8 Sn6 W48
• Calculated formula: K11.04 O196.24 P8 Sn5.976 W48
• Title of publication: Tin(ii)-functionalization of the archetypal {P8W48} polyoxotungstate.
• Authors of publication: Izarova, N. V.; Klaß, L; de Oliveira, P.; Mbomekalle, I.-M.; Peters, V.; Haarmann, F.; Kögerler, P
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 44
• Pages of publication: 19200 - 19206
• a: 26.9749 ± 0.0003 Å
• b: 26.9749 ± 0.0003 Å
• c: 21.0538 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 15319.7 ± 0.3 ų
• Cell temperature: 120 ± 0.1 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 139
• Hermann-Mauguin space group symbol: I 4/m m m
• Hall space group symbol: -I 4 2
• Residual factor for all reflections: 0.1141
• Residual factor for significantly intense reflections: 0.0785
• Weighted residual factors for significantly intense reflections: 0.1905
• Weighted residual factors for all reflections included in the refinement: 0.2117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No