Information card for entry 7037197

Structure parameters

• Common name: tetramethylammonium rhodium nonaniobate
• Formula: C24 H100 N6 Nb8.88 O42 Rh1.12
• Calculated formula: C24 H100 N6 Nb8.876 O42 Rh1.124
• Title of publication: Two Rh(III)-substituted polyoxoniobates and their base-induced transformation: [H2RhNb9O28](6-) and [Rh2(OH)4Nb10O30](8.).
• Authors of publication: Son, Jung-Ho; Casey, Willam H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 47
• Pages of publication: 20330 - 20333
• a: 11.123 ± 0.0008 Å
• b: 12.1932 ± 0.0009 Å
• c: 13.3388 ± 0.001 Å
• α: 85.961 ± 0.001°
• β: 68.004 ± 0.001°
• γ: 87.862 ± 0.001°
• Cell volume: 1673.1 ± 0.2 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.036
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0825
• Weighted residual factors for all reflections included in the refinement: 0.084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No