Rare-earth metal bis(silylamide) complexes supported by mono-dentate arylamido ligand: synthesis, reactivity, and catalyst precursors in living cis-1,4-selective polymerization of isoprene.
Authors of publication
Shi, Liqin; Su, Qi; Chen, Jue; Li, Xiaonian; Luo, Yunjie
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2016
Journal volume
45
Journal issue
4
Pages of publication
1391 - 1397
a
10.9004 ± 0.00017 Å
b
17.234 ± 0.0002 Å
c
21.1886 ± 0.0003 Å
α
90°
β
102.427 ± 0.0015°
γ
90°
Cell volume
3887.17 ± 0.1 Å3
Cell temperature
223 ± 2 K
Ambient diffraction temperature
223 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0311
Residual factor for significantly intense reflections
0.025
Weighted residual factors for significantly intense reflections
0.0577
Weighted residual factors for all reflections included in the refinement
0.0598
Goodness-of-fit parameter for all reflections included in the refinement
