Information card for entry 7037880

Structure parameters

• Formula: C73 H128 P4 Si10.8 Th2
• Calculated formula: C72.9978 H127.999 P3.9998 Si10.8 Th2
• Title of publication: White phosphorus activation by a Th(iii) complex.
• Authors of publication: Formanuik, Alasdair; Ortu, Fabrizio; Beekmeyer, Reece; Kerridge, Andrew; Adams, Ralph W.; Mills, David P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 6
• Pages of publication: 2390 - 2393
• a: 21.10705 ± 0.00017 Å
• b: 21.10705 ± 0.00017 Å
• c: 21.10705 ± 0.00017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9403.35 ± 0.13 ų
• Cell temperature: 150.02 ± 0.1 K
• Ambient diffraction temperature: 150.02 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 205
• Hermann-Mauguin space group symbol: P a -3
• Hall space group symbol: -P 2ac 2ab 3
• Residual factor for all reflections: 0.0834
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.1685
• Weighted residual factors for all reflections included in the refinement: 0.1918
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No