Information card for entry 7038533

Structure parameters

• Formula: C34 H47 K O7 Si Te
• Calculated formula: C34 H47 K O7 Si Te
• SMILES: [Te]([K]12345([O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6)[O]1CCCC1)[Si](c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Synthesis and characterization of potassium aryl- and alkyl-substituted silylchalcogenolate ligands.
• Authors of publication: Brown, Jessie L.; Montgomery, Ashley C.; Samaan, Christopher A.; Janicke, Michael T.; Scott, Brian L.; Gaunt, Andrew J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 24
• Pages of publication: 9841 - 9852
• a: 9.2562 ± 0.0019 Å
• b: 10.431 ± 0.002 Å
• c: 19.332 ± 0.004 Å
• α: 99.814 ± 0.002°
• β: 93.297 ± 0.002°
• γ: 96.939 ± 0.002°
• Cell volume: 1819.9 ± 0.6 ų
• Cell temperature: 140 ± 1 K
• Ambient diffraction temperature: 140 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0261
• Residual factor for significantly intense reflections: 0.0231
• Weighted residual factors for significantly intense reflections: 0.0571
• Weighted residual factors for all reflections included in the refinement: 0.0585
• Goodness-of-fit parameter for all reflections included in the refinement: 1.231
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No